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1,2-Dinitrobenzene → HCID 13292704、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,2-Dinitrobenzene | HCID 10707 | — |
| 反応物 | Diethyl methylphosphonite | HCID 85063 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | HCID 13292704 | HCID 13292704 | — |
反応手順
A mixture of 1,2-dinitrobenzene (2.48 mmol), diethyl methylphosphonite (3.72 mmol) and acetonitrile (3 ml) is stirred at RT overnight. The reaction is concentrated to dryness, and the residue is purified by preparative thin layer chromatography (TLC) to yield ethyl P-methyl-2-nitrophenyl-phosphinate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04520197 |
| 出典データセット | uspto-grants-1985_05 |
| ORD ID | ord-c34ce62fdba4431e8122437a12d3da68 |
| 出典メモ | uspto-grants-1985_05 |