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Hydrochloric Acid → 4-chloro-5-(2,4-dichlorophenoxy)benzo-2,1,3-oxadiazole N-oxide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 2-Chloro-3-(2,4-dichlorophenoxy)-6-nitroaniline | HCID 20264344 | — |
| 反応物 | N-methylcarbonyl 2-chloro-3-(2,4-dichlorophenoxy)-6-nitroaniline | HCID 20264352 | — |
| 反応物 | Sodium Hypochlorite | HCID 23665760 | — |
| 生成物 | 4-chloro-5-(2,4-dichlorophenoxy)benzo-2,1,3-oxadiazole N-oxide | HCID 53750274 | — |
反応手順
Following the procedure of Example 4, N-methylcarbonyl 2-chloro-3-(2,4-dichlorophenoxy)-6-nitroaniline is converted, by reaction with HCl, to 2-chloro-3-(2,4-dichlorophenoxy)-6-nitroaniline, which is then reacted with potassium hydroxide and sodium hypochlorite, again following Example 4 procedures, to yield the final product, 4-chloro-5-(2,4-dichlorophenoxy)benzo-2,1,3-oxadiazole N-oxide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04544400 |
| 出典データセット | uspto-grants-1985_10 |
| ORD ID | ord-04bce43b8f9d420aa740cc9c2e7931dd |
| 出典メモ | uspto-grants-1985_10 |