化工社化工社 化学情報印刷レポート · 研究参考用
Benzyl Alcohol → HCID 178476834、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzyl Alcohol | HCID 244 | — |
| 反応物 | Water | HCID 962 | — |
| 反応物 | HCID 178476830 | HCID 178476830 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | HCID 178476834 | HCID 178476834 | 91.2% |
反応手順
A solution of α-hydroxyethylphosphinic acid (5.5 g) and benzyl alcohol (2.26 g) in benzene (50 ml) was heated for 8 hours with removal of water through a Dean-Stark apparatus. After cooling, the reaction mixture was washed with water, dried over magnesium sulfate and concentrated in vacuo to give 3.65 g (91.2%) of benzyl α-hydroxyethylphosphinate (Compound No. 36).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04544652 |
| 出典データセット | uspto-grants-1985_10 |
| ORD ID | ord-3b10e5d9b7a94dba8dfc894d8aea4436 |
| 出典メモ | uspto-grants-1985_10 |