関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ethanolamine | HCID 700 | — |
| 反応物 | 2-cyanomethyl-N-phenylphthalimide | HCID 20265457 | — |
| 生成物 | Phenylglycine nitrile | HCID 76307 | — |
反応手順
100 g of 2-cyanomethyl-N-phenylphthalimide were introduced, a little at a time, into 100 g of monoethanolamine at 80° C. After 10 minutes, the mixture was cooled to 20° C., and 400 g of ice water were added dropwise. The precipitated product was filtered off under suction and washed neutral with ice water.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04544755 |
|---|
| 出典データセット | uspto-grants-1985_10 |
|---|
| ORD ID | ord-7c7b2faa11fd4a8da8c7465902762202 |
|---|
| 出典メモ | uspto-grants-1985_10 |
|---|
