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Isopropylamine → HCID 13458391、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isopropylamine | HCID 6363 | — |
| 反応物 | 4'-Chloroacetyl(acetanilide) | HCID 8805 | — |
| 反応物 | 1,4-Dioxane | HCID 31275 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 13458391 | HCID 13458391 | 89.6% |
反応手順
In a reactor, 21 g (0.1 mol) of 4-acetylaminophenacyl chloride are introduced into a mixture comprising 100 ml of dioxane, 26 ml (0.3 mol) of isopropylamine and 20 ml of water. The reaction medium is stirred at 30°-40° C. for 2 hours. After the addition of 500 ml of iced water, a precipitate is collected, washed and dried. Recrystallization from ethyl acetate gives 21 g of N-(4-acetylaminophenacyl)isopropylamine, which is in the form of a white powder. Melting point (inst.)=156° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04545996 |
| 出典データセット | uspto-grants-1985_10 |
| ORD ID | ord-4808f652adcb49a78b550fd4286098fc |
| 出典メモ | uspto-grants-1985_10 |