関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Triphenylphosphine | HCID 11776 | — |
| 反応物 | Chloromethyl ethyl ether | HCID 18523 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | (Ethoxymethyl)(triphenyl)phosphanium chloride | HCID 21470303 | — |
反応手順
A solution of 99.66 g of triphenylphosphine and 37.82 g of chloromethyl ethyl ether in 240 ml of dry benzene was stirred and refluxed (84° C.) for 6 hours. The mixture then was chilled and filtered to give 7, as a white solid, mp 205°-206° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04173463 |
|---|
| 出典データセット | uspto-grants-1979_11 |
|---|
| ORD ID | ord-3204c8b2736246ee820e2cf7f1906092 |
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| 出典メモ | uspto-grants-1979_11 |
|---|
