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HRID 46430作成日:2026年10月25日

Acetic Acid → Acetanilide

https://huagongshe.com/reaction/46430

反応式

関与物質

役割名称HCID仕込み量
反応物Acetic AcidHCID 176—
反応物AnilineHCID 6115—
反応物PhosphoniumHCID 5460504—
生成物AcetanilideHCID 90420%

反応手順

To the same reaction mixture containing the phosphonium salt as in Example 1 was added a mixture of 3.0 g. (0.05 mole) of acetic acid and 5.2 g. (0.056 mole) of aniline, and the resulting mixture was reacted under reflux for 2 hours. Thereafter, the same aftertreatment as in Example 1 was effected to obtain acetanilide, yield 20% based on acetic acid.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04173563
出典データセットuspto-grants-1979_11
ORD IDord-5125bfbe373845828fb7c1f366821596
出典メモuspto-grants-1979_11