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Acetic Acid → Acetanilide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | Phosphonium | HCID 5460504 | — |
| 生成物 | Acetanilide | HCID 904 | 20% |
反応手順
To the same reaction mixture containing the phosphonium salt as in Example 1 was added a mixture of 3.0 g. (0.05 mole) of acetic acid and 5.2 g. (0.056 mole) of aniline, and the resulting mixture was reacted under reflux for 2 hours. Thereafter, the same aftertreatment as in Example 1 was effected to obtain acetanilide, yield 20% based on acetic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04173563 |
| 出典データセット | uspto-grants-1979_11 |
| ORD ID | ord-5125bfbe373845828fb7c1f366821596 |
| 出典メモ | uspto-grants-1979_11 |