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N-Methylaniline → N-Methylacetanilide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-Methylaniline | HCID 7515 | — |
| 反応物 | Dipropan-2-yl hydrogen phosphite | HCID 558181 | — |
| 生成物 | N-Methylacetanilide | HCID 11364 | 53% |
反応手順
Example 34 was repeated, except that 0.05 mole of phosphorous diisopropyl ester was used in place of phosphorous monoethyl ester and 0.05 mole of N-methylaniline was used in place of aniline, to obtain N-methylacetanilide, yield 53% based on N-methylaniline.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04173563 |
| 出典データセット | uspto-grants-1979_11 |
| ORD ID | ord-000eec09122c4356b22814905c4f1863 |
| 出典メモ | uspto-grants-1979_11 |