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Thiophenol → N-benzyloxycarbonyl-glycine-phenythio ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thiophenol | HCID 7969 | — |
| 反応物 | Benzyloxycarbonylglycine | HCID 14349 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | N-benzyloxycarbonyl-glycine-phenythio ester | HCID 22764889 | 62% |
反応手順
Using thiophenol and Z-Gly.OH, Example 78 was repeated; except that dichloromethane was used in place of ethyl acetate as the extraction solvent, to obtain N-benzyloxycarbonyl-glycine-phenythio ester (hereinafter represented by ##STR12## in a yield of 62%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04173563 |
| 出典データセット | uspto-grants-1979_11 |
| ORD ID | ord-01bd8ea14e7b4957854705e522f04f34 |
| 出典メモ | uspto-grants-1979_11 |