化工社化工社 化学情報印刷レポート · 研究参考用
Trifop → HCID 13505617、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Trifop | HCID 181206 | — |
| 反応物 | 2,5-Dichlorobenzene-1-sulfonyl isocyanate | HCID 12875187 | — |
| 生成物 | HCID 13505617 | HCID 13505617 | — |
反応手順
A solution of one gram (0.0031 mole) 2-[4-(4-trifluoromethylphenoxy)phenoxy]-propionic acid in dry CHCH3 was treated with 0.8 gram (g) (0.0081 mole) 2,5-dichlorobenzene sulfonyl isocyanate. The solution was stirred for approximately 18 hours, then heated to reflux for three hours, followed by cooling.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04549901 |
| 出典データセット | uspto-grants-1985_10 |
| ORD ID | ord-1964ed97a263462cb25e4e9a6d4bd11f |
| 出典メモ | uspto-grants-1985_10 |