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HRID 465165作成日:2026年10月26日

Hexachlorocyclotriphosphazene → Trichlorotriphenoxycyclotriphosphazene

https://huagongshe.com/reaction/465165

反応式

関与物質

役割名称HCID仕込み量
反応物HexachlorocyclotriphosphazeneHCID 220225—
反応物Phenolate SodiumHCID 4445035—
生成物TrichlorotriphenoxycyclotriphosphazeneHCID 23418754—

反応手順

Examples 8 to 12 below illustrate embodiments of the invention in which hexachlorocyclotriphosphazene (compound 1) is reacted first with sodium phenoxide to produce an intermediate (trischlorotrisphenoxycyclotriphosphazene), 19 which is then reacted without separation with sodium 4-nitrophenoxide to afford tris(4-nitrophenoxy)tris(phenoxy)cyclotriphosphazene 20. The nitro groups of 20 are reduced to afford the corresponding tris amino compound 21 which is then used according to Scheme I or Scheme II shown in FIG. 2 and FIG. 3, respectively.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04550177
出典データセットuspto-grants-1985_10
ORD IDord-142809559af4447d878cb8abbe1f5e41
出典メモuspto-grants-1985_10