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Ethanol → 2-Methoxybenzoylacetonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Sodium Cyanide | HCID 8929 | — |
| 反応物 | Bromomethyl 2-methoxyphenyl ketone | HCID 123440 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 2-Methoxybenzoylacetonitrile | HCID 4962750 | — |
反応手順
A 10.0 g. portion of α-bromo-o-methoxyacetophenone is suspended in 50 ml. of ethanol. A solution of 6.4 g. of sodium cyanide in 30 ml. of water is added as described in Example 38. Following the procedure of Example 38, there is obtained o-methoxybenzoylacetonitrile.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04173650 |
| 出典データセット | uspto-grants-1979_11 |
| ORD ID | ord-c92257dc890c478997046b240e38ba71 |
| 出典メモ | uspto-grants-1979_11 |