反応式
Br[CH2:2][C:3]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[O:11][CH3:12])=[O:4].C(O)C.[C-:16]#[N:17].[Na+]>O>[CH3:12][O:11][C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=1[C:3]([CH2:2][C:16]#[N:17])=[O:4]参加物
5
実験手順
A 10.0 g. portion of α-bromo-o-methoxyacetophenone is suspended in 50 ml. of ethanol. A solution of 6.4 g. of sodium cyanide in 30 ml. of water is added as described in Example 38. Following the procedure of Example 38, there is obtained o-methoxybenzoylacetonitrile.
出典と根拠
- ORDレコード
- ord-c92257dc890c478997046b240e38ba71
- 出典データセット
- uspto-grants-1979_11
- 特許番号
- US04173650
関連ノート
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