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Isothiocyanic acid, p-dimethylaminophenyl ester → N-(2,6-Diethylphenyl)-2-[[[[4-(dimethylamino)phenyl]amino]thioxomethyl](diphenylmethyl)amino]acetamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isothiocyanic acid, p-dimethylaminophenyl ester | HCID 75047 | — |
| 反応物 | N-[2,6-bis(1-Methylethyl)phenyl]-2-[(diphenylmethyl)amino]acetamide | HCID 1645639 | — |
| 反応物 | N-[2,6-bis(1-Methylethyl)phenyl]-2-[(2,2-diphenylethyl)amino]acetamide | HCID 19874997 | — |
| 生成物 | N-(2,6-Diethylphenyl)-2-[[[[4-(dimethylamino)phenyl]amino]thioxomethyl](diphenylmethyl)amino]acetamide | HCID 19874867 | — |
反応手順
When in the procedure of Example 80 an appropriate amount of 4-dimethylaminophenylisothiocyanate was substituted for ethyl isocyanato acetate and an appropriate amount of the product of Example 4 was substituted for the product of Example 70 and the general procedure of Example 80 was followed the title compound was obtained. Total yield, 0.68 g (62%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05153226 |
| 出典データセット | uspto-grants-1992_10 |
| ORD ID | ord-2c9899b9226d41c5bb67574309d31e3a |
| 出典メモ | uspto-grants-1992_10 |