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3,4,5-Trimethoxybenzaldehyde → N,N-Dimethyl-N'-[(3,4,5-trimethoxyphenyl)methylene]-1,3-propanediamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,4,5-Trimethoxybenzaldehyde | HCID 6858 | — |
| 反応物 | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | N,N-Dimethyl-N'-[(3,4,5-trimethoxyphenyl)methylene]-1,3-propanediamine | HCID 20386241 | 94% |
反応手順
Interaction of 21 g of 3,4,5-trimethoxybenzaldehyde with 11 g of 3-dimethylaminopropylamine in 80 ml. of benzene following the procedure described in Example 1 yields 28.2 g of product as an oil, boiling point 162°-167° C. at 0.4-0.5 mm. of Hg.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04174317 |
| 出典データセット | uspto-grants-1979_11 |
| ORD ID | ord-4b3cc334fad24d0e82410294c773b13e |
| 出典メモ | uspto-grants-1979_11 |