化工社化工社 化学情報印刷レポート · 研究参考用
Butyltin trichloride → Dibutyltin dichloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Butyltin trichloride | HCID 14236 | — |
| 反応物 | Butyltricyclohexylstannane | HCID 81516 | — |
| 溶媒 | O-Xylene | HCID 7237 | — |
| 生成物 | Dibutyltin dichloride | HCID 12688 | — |
| 生成物 | Stannane, chlorotricyclohexyl- | HCID 76539 | — |
反応手順
A solution of equimolar amounts of butyl tricyclohexyltin and butyltin trichloride in commercial xylene was refluxed for 221/2 hours. Analysis of the reaction mixture obtained showed that the reaction had gone to about 89% completion to form predominantly tricyclohexyltin chloride and dibutyltin dichloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04174346 |
| 出典データセット | uspto-grants-1979_11 |
| ORD ID | ord-c5e415f74b814fec966c82cbe051672a |
| 出典メモ | uspto-grants-1979_11 |