化工社化工社 化学情報印刷レポート · 研究参考用
Hexanoic Acid → 7-Methyl-2-pentyl-3H-imidazo[4,5-b]pyridine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hexanoic Acid | HCID 8892 | — |
| 反応物 | 4-Methylpyridine-2,3-diamine | HCID 317495 | — |
| 生成物 | 7-Methyl-2-pentyl-3H-imidazo[4,5-b]pyridine | HCID 19814121 | — |
反応手順
The title compound was prepared from 2,3-diamino-4-picoline (0.246 g, 2 mmol) and hexanoic acid (0.25 ml, 2 mmols) according to the procedure described in Step 1 of Example 9. The crude product was purified by flash chromatography on silica-gel using EtOAc-MeOH (9:1) to give the pure product (0.28 g, 69%) as a tan colored solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05157026 |
| 出典データセット | uspto-grants-1992_10 |
| ORD ID | ord-841ec3cba52e428982d1c07469bac46d |
| 出典メモ | uspto-grants-1992_10 |