関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | Styrene | HCID 7501 | — |
| 生成物 | gamma-Phenyl-gamma-butyrolactone | HCID 13884 | 70% |
反応手順
Styrene in the amount of 20 grams was dissolved in 100 milliliters of acetic acid containing 10% potassium acetate. Ceric acetate in the amount of 0.005 mole was added and the reaction mixture was heated in a sealed tube at 110° C. overnight. The lactone, gamma-phenyl butyrolactone, was obtained in 70% yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04175089 |
|---|
| 出典データセット | uspto-grants-1979_11 |
|---|
| ORD ID | ord-3382055977444d27a94c974baede3424 |
|---|
| 出典メモ | uspto-grants-1979_11 |
|---|
