化工社化工社 化学情報印刷レポート · 研究参考用
1-Octene → Gamma-Decalactone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Octene | HCID 8125 | — |
| 反応物 | Potassium Acetate | HCID 517044 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | Gamma-Decalactone | HCID 12813 | 61% |
反応手順
Octene-1 in an amount of 2.24 g. and 5.1 g. of Mn2O3 (comprising two equivalents of Mn+3 based on titration value) were refluxed under nitrogen in 200 ml. glacial acetic acid containing 60 g. potassium acetate. After a period of less than two hours, gamma-n-hexyl-butyrolactone was obtained in a yield of 61%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04175089 |
| 出典データセット | uspto-grants-1979_11 |
| ORD ID | ord-43204c96c25d493ba43892f30698f076 |
| 出典メモ | uspto-grants-1979_11 |