化工社化工社 化学情報印刷レポート · 研究参考用
Water → Epiandrosterone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 3beta-Acetoxy-5alpha-androstan-17-one | HCID 908740 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Epiandrosterone | HCID 441302 | 95% |
反応手順
A mixture of 5 (1 g, 3.00 mmol), NaOH 0.12 g (3.44 mmol) in methanol was refluxed for 10 min, cooled to room temperature and treated with water. The resulting precipitate was filtered off and washed with water to afford crude product 6 (0.82 g, 95%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08623849B2 |
| 出典データセット | uspto-grants-2014_01 |
| ORD ID | ord-ae5f46f7bef043fb87e21b3a77341060 |
| 出典メモ | uspto-grants-2014_01 |