化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → HCID 178421680、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Thiocarbohydrazide | HCID 2724189 | — |
| 反応物 | (1-Methylcyclopropyl)-glyoxylic acid tert-butylamide | HCID 20385839 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178421680 | HCID 178421680 | — |
反応手順
183 grams of (1-methyl-cyclopropyl)-glyoxalic acid-tert.-butylamide and 112 grams of thiocarbohydrazide were added to a mixture of 1 liter of 1 normal HCl and 1 liter of ethanol. The mixture was boiled under reflux for 8 hours, cooled, diluted with 2 liters of water and the crystals filtered off with suction. There were obtained white crystals with a yellow luster which were dried.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04175188 |
| 出典データセット | uspto-grants-1979_11 |
| ORD ID | ord-e471648b4ae44be4b25f0eae45b4618f |
| 出典メモ | uspto-grants-1979_11 |