化工社化工社 化学情報印刷レポート · 研究参考用
Thionyl Chloride → 3,5-Difluorobenzoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 3,5-Difluorobenzoic acid | HCID 101265 | — |
| 生成物 | 3,5-Difluorobenzoyl chloride | HCID 145600 | — |
反応手順
1.63 g (10.00 mmol) 3,5-difluoro-benzoic acid were mixed with 20 mL thionyl chloride and boiled for 2 h. The reaction mixture was evaporated to dryness and coevaporated twice with toluene. The residue was reacted further as the crude product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08629137B2 |
| 出典データセット | uspto-grants-2014_01 |
| ORD ID | ord-a565cd0d833a42f3b36e645c6b592ea7 |
| 出典メモ | uspto-grants-2014_01 |