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Phenol → 4-Hydroxyphenylglycine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenol | HCID 996 | — |
| 反応物 | Ammonium Acetate | HCID 517165 | — |
| 反応物 | Potassium glyoxylate | HCID 23669142 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 4-Hydroxyphenylglycine | HCID 92143 | 33.6% |
反応手順
42.1 g of potassium glyoxylate, 75 g of ammonium acetate, 60 g of phenol and 130 ml of water are treated in the same manner as described in Example 1. The reaction was conducted for a period of 24 hours. 18.1 g of DL-p-hydroxyphenylglycine are thereby obtained as crystals. Yield 33.6%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04175206 |
| 出典データセット | uspto-grants-1979_11 |
| ORD ID | ord-8f6516e5171a4007993cfba8ee8e628f |
| 出典メモ | uspto-grants-1979_11 |