化工社化工社 化学情報印刷レポート · 研究参考用
Phenol → 4-Hydroxyphenylglycine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenol | HCID 996 | — |
| 反応物 | Ammonium formate | HCID 2723923 | — |
| 反応物 | Sodium glyoxylate | HCID 23662273 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 4-Hydroxyphenylglycine | HCID 92143 | 34.2% |
反応手順
36.9 g of sodium glyoxylate, 61.3 g of ammonium formate, 60 g of phenol and 130 g of water are treated in the same manner as described in Example 1. 18.5 g of DL-p-hydroxyphenylglycine are thereby obtained as crystals. Yield: 34.2% M.p. 225°-228° C. (decomp.).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04175206 |
| 出典データセット | uspto-grants-1979_11 |
| ORD ID | ord-6568d7eac24a4c50a34ceef5bb51d78a |
| 出典メモ | uspto-grants-1979_11 |