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HRID 470159作成日：2026年10月26日
Triethylamine → 4-[N-(3-Methoxy-benzoyl)-hydrazino]-7-methyl-2-oxo-1,5-diphenyl-1,2,5,8-tetrahydro-pyrido[2,3-d]pyrimidine-6-carboxylic acid ethyl ester
https://huagongshe.com/reaction/470159
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | m-Anisohydrazide | HCID 79848 | — |
| 反応物 | 4-Chloro-7-methyl-2-oxo-1,5-diphenyl-1,2,5,8-tetrahydro-pyrido[2,3-d]pyrimidine-6-carboxylic acid ethyl ester | HCID 67514848 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 4-[N-(3-Methoxy-benzoyl)-hydrazino]-7-methyl-2-oxo-1,5-diphenyl-1,2,5,8-tetrahydro-pyrido[2,3-d]pyrimidine-6-carboxylic acid ethyl ester | HCID 67969325 | — |
反応手順
The compound of step 6 (100 mg, 0.237 mmol) was taken in 2 ml EtOH and treated successively with m-anisic hydrazide (99.6 mg, 0.6 mmol) and TEA (Triethylamine) (35 microl, 0.25 mmol) at room temperature and stirred at 60° C. for 72 h.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US08629272B2 |
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| 出典データセット | uspto-grants-2014_01 |
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| ORD ID | ord-f9f018ebeb474dff84a404c8b1998c16 |
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| 出典メモ | uspto-grants-2014_01 |
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