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1-(4-Bromo-3-methylphenyl)ethanone → (R)-2-methyl-propane-2-sulfinic acid [1-(4-bromo-3-methyl-phenyl)ethylidene]-amide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-(4-Bromo-3-methylphenyl)ethanone | HCID 347124 | — |
| 反応物 | tert-Butylsulfinamide, (R)-(+)- | HCID 10964479 | — |
| 反応物 | 6-cyclopropyl-6-(2-hydroxy-2-methylpropyl)-3-((S)-1-(4-(1-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenyl)ethyl)-1,3-oxazinan-2-one | HCID 59635673 | — |
| 生成物 | (R)-2-methyl-propane-2-sulfinic acid [1-(4-bromo-3-methyl-phenyl)ethylidene]-amide | HCID 86649415 | — |
反応手順
The title compound was prepared from 1-(4-bromo-3-methyl-phenyl)-ethanone and (R)-2-methyl-2-propanesulfinamide following a procedure analogous to that described in Step 1 of Intermediate 1. Mass spectrum (ESI+): m/z=316/318 (Br) [M+H]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08629138B2 |
| 出典データセット | uspto-grants-2014_01 |
| ORD ID | ord-85fb8f10ff7e4251b8d4fcde08ad75a4 |
| 出典メモ | uspto-grants-2014_01 |