化工社化工社 化学情報印刷レポート · 研究参考用
Dimethylformamide → N,N-dimethyl-2-(3-cyano-2-pyridyl) ethenamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethylformamide | HCID 6228 | — |
| 反応物 | 2-Methylpyridine-3-carbonitrile | HCID 4738308 | — |
| 生成物 | N,N-dimethyl-2-(3-cyano-2-pyridyl) ethenamine | HCID 54435625 | — |
反応手順
N,N-dimethyl-2-(3-cyano-2-pyridyl)ethenamine was prepared using the procedure of 4 A from 2-methyl-3-cyanopyridine (9.0 g, 0.076 m), DMF acetal (11.0 g, 0.092 m) and DMF (50 mL) yielding N,N-dimethyl-2-(3-cyano-2-pyridyl) ethenamine b.p.=133°-135° (0.3 mm), m.p.=49°-50° after sublimation at 50° (0.3 mm).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04176183 |
| 出典データセット | uspto-grants-1979_11 |
| ORD ID | ord-4a2635ef6c464657ae9922b89defc428 |
| 出典メモ | uspto-grants-1979_11 |