化工社化工社 化学情報印刷レポート · 研究参考用
4-Ethylpyridin-2-amine → 4-Ethyl-5-iodopyridin-2-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Ethylpyridin-2-amine | HCID 118425 | — |
| 反応物 | N-Iodosuccinimide | HCID 120273 | — |
| 生成物 | 4-Ethyl-5-iodopyridin-2-amine | HCID 58200578 | — |
反応手順
The title compound is synthesized according to general procedure GP1 starting from 5.0 g (41 mmol) 4-ethyl-pyridin-2-ylamine and 9.2 g (41 mmol) NIS. Yield after precipitation from the reaction mixture and isolation of additional product from the mother liquid by chromatography using silica gel: 10.3 g (100%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08633183B2 |
| 出典データセット | uspto-grants-2014_01 |
| ORD ID | ord-2c7b77c81fe6431e91dfa4bc4768f366 |
| 出典メモ | uspto-grants-2014_01 |