2,2-Dimethylethenylboronic acid → N-(2-Cyano-4-(2-methylprop-1-enyl)phenyl)sulfamide

反応式

[C:1]([C:3]1[CH:8]=[C:7](Br)[CH:6]=[CH:5][C:4]=1[NH:10][S:11]([NH2:14])(=[O:13])=[O:12])#[N:2].[CH3:15][C:16]([CH3:21])=[CH:17]B(O)O>>[C:1]([C:3]1[CH:8]=[C:7]([CH:15]=[C:16]([CH3:21])[CH3:17])[CH:6]=[CH:5][C:4]=1[NH:10][S:11]([NH2:14])(=[O:13])=[O:12])#[N:2]

参加物

反応物 2

HCID 27632992,2-Dimethylethenylboronic acid

HCID 67402187N-(2-cyano-4-bromophenyl)sulfamide

生成物 1

HCID 67397727N-(2-Cyano-4-(2-methylprop-1-enyl)phenyl)sulfamide

実験手順

Prepared as in Example 77a from N-(2-cyano-4-bromophenyl)sulfamide (Example 83b) and 2-methylprop-1-enylboronic acid.

出典と根拠

ORDレコード: ord-49ffb972738641268f9c28fd2d724143
出典データセット: uspto-grants-2014_01
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08633186B2

反応ノート

読み込み中…