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HRID 47531作成日:2026年10月25日

Hydroxyacetone → 2-Propanone, 1-((methylsulfonyl)oxy)-

https://huagongshe.com/reaction/47531

反応式

関与物質

役割名称HCID仕込み量
反応物HydroxyacetoneHCID 8299—
反応物Methanesulfonyl chlorideHCID 31297—
反応物Sodium BicarbonateHCID 516892—
溶媒ChloroformHCID 6212—
生成物2-Propanone, 1-((methylsulfonyl)oxy)-HCID 146754—

反応手順

Thirty-seven (37) mg of hydroxyacetone was dissolved in 2 ml of chloroform, and to which 0.078 ml of methanesulfonyl chloride was added. After stirring the reaction liquid at room temperature for 30 minutes, saturated aqueous sodium bicarbonate solution was added and extracted with chloroform. The extract was dried over anhydrous sodium sulfate and concentrated to provide the title compound.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06699880B1
出典データセットuspto-grants-2004_03
ORD IDord-ae0dc196daec479296ba40aa26395f87
出典メモuspto-grants-2004_03