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HRID 476542作成日:2026年10月26日

Platinous chloride → HCID 178435846、化合物

https://huagongshe.com/reaction/476542

反応式

関与物質

役割名称HCID仕込み量
反応物Platinous chlorideHCID 2770—
反応物HCID 178435845HCID 178435845—
溶媒DimethylformamideHCID 6228—
生成物HCID 178435846HCID 178435846—

反応手順

In a suitable 150 ml vessel 50 ml of dimethylformamide is brought to reflux and 20 mg 5-bromo octaethylporphine free base is added and dissolved. To this solution 8 mg platinum chloride is added and permitted to react for about 20 minutes. Thereafter, the reaction mixture is permitted to cool and crystal formation promoted by the addition of 50 ml distilled water. The reaction mixture is allowed to sit for about twenty four hours to increase crystal size. The reaction mixture is filtered by vacuum filtration and the solids retained.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04885114
出典データセットuspto-grants-1989_12
ORD IDord-f01890c04f3b4fe4939f16b4f5a0396c
出典メモuspto-grants-1989_12