(R)-Dihydromaleimide → HCID 19838062、化合物
反応式
[OH:1][CH:2]1[NH:6][C:5](=[O:7])[CH:4]=[CH:3]1>C(O)CCC>[CH2:2]([O:1][CH:2]1[NH:6][C:5](=[O:7])[CH:4]=[CH:3]1)[CH2:3][CH2:4][CH3:5]参加物
3
反応条件
- 温度
- 70 °C
実験手順
A mixture of 2.5 g of 1,5-dihydro-5-hydroxy-2H-pyrrol-2-one in 75 cm3 of 1-butanol and 1.3 g of Amberlite IR 120 H is heated to 70° C. for 2 hours. After allowing to return to ambient temperature, the residue is filtered and the solvent is evaporated under reduced pressure. 3.9 g of the expected product is obtained.
後処理
- customto return to ambient temperature
- filtrationthe residue is filtered
- customthe solvent is evaporated under reduced pressure
出典と根拠
- ORDレコード
- ord-99bc030f154b4f6a83c861dcbe114683
- 出典データセット
- uspto-grants-1989_12
- 特許番号
- US04885307
反応ノート
読み込み中…