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(5-Aminopentyl)diethylamine → P,P-bis(2,2-dimethyl-1-aziridinyl)-N-(5-diethylamino-1-pentyl)-phosphinic amide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (5-Aminopentyl)diethylamine | HCID 4584949 | — |
| 反応物 | P,P-bis(2,2-dimethyl-1-aziridinyl)phosphinyl chloride | HCID 13511140 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | P,P-bis(2,2-dimethyl-1-aziridinyl)-N-(5-diethylamino-1-pentyl)-phosphinic amide | HCID 19836605 | 90% |
反応手順
In a similar manner 0.025 moles of P,P-bis(2,2-dimethyl-1-aziridinyl)phosphinoyl chloride in about 170 mL of THF are treated by dropwise addition with 0.026 moles of 5-diethylaminopentylamine in 25 mL of THF, stirred for several hours at ambient temperature, filtered, concentrated by rotary evaporation and vacuum distilled to yield about 90% pure P,P-bis(2,2-dimethyl-1-aziridinyl)-N-(5-diethylamino-1-pentyl)-phosphinic amide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04886790 |
| 出典データセット | uspto-grants-1989_12 |
| ORD ID | ord-9aef35d6daf64598af0ba4a421975c18 |
| 出典メモ | uspto-grants-1989_12 |