化工社化工社 化学情報印刷レポート · 研究参考用
Ammonia → 2-Amino-1-phenoxy-propene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | p-Toluenesulfonic acid | HCID 6101 | — |
| 反応物 | 1-Phenoxy-2-propanone | HCID 69313 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | 2-Amino-1-phenoxy-propene | HCID 70048860 | — |
反応手順
0.2 mol of phenoxyacetone in 200 ml of tetrahydrofuran is saturated at reflux temperature with ammonia gas with the addition of 0.2 g of p-toluene sulphonic acid. The mixture is allowed to stand at room temperature for 24 hours and the solvent is then removed by evaporation in vacuo. The evaporation residue is employed crude in the reaction of Example 5B.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04886804 |
| 出典データセット | uspto-grants-1989_12 |
| ORD ID | ord-f9508f221bf3480cacb1d5f539bc49be |
| 出典メモ | uspto-grants-1989_12 |