化工社化工社 化学情報印刷レポート · 研究参考用
Methyl Salicylate → Trimethylolethane salicylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl Salicylate | HCID 4133 | — |
| 反応物 | Trimethylolethane | HCID 6502 | — |
| 反応物 | 2,3-Dihydroxypropyl salicylate | HCID 3849318 | — |
| 反応物 | Sodium Methoxide | HCID 10942334 | — |
| 生成物 | Trimethylolethane salicylate | HCID 70390081 | — |
反応手順
Trimethylolethane salicylate was prepared by the method described in Example 1 for the preparation of glycerol salicylate except that the reactants were trimethylolethane (60.1 g; 0.5 moles), methyl salicylate (119.7 g; 0.788 moles), sodium methoxide (0.82 g; 0.015 moles). The final methyl salicylate level was 10.0%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04886843 |
| 出典データセット | uspto-grants-1989_12 |
| ORD ID | ord-7cf1c8d830fe483db8fd085ee7f9672d |
| 出典メモ | uspto-grants-1989_12 |