Chlorosuccinimide → HCID 15017527、化合物

反応式

[Br:1][C:2]1[C:8]([Cl:9])=[CH:7][C:5]([NH2:6])=[C:4]([CH3:10])[CH:3]=1.[Cl:11]N1C(=O)CCC1=O>>[Br:1][C:2]1[CH:3]=[C:4]([CH3:10])[C:5]([NH2:6])=[C:7]([Cl:11])[C:8]=1[Cl:9]

参加物

反応物 2

HCID 31398Chlorosuccinimide

HCID 71720264-bromo-5-chloro-2-methylaniline

生成物 1

HCID 15017527HCID 15017527、化合物

実験手順

This material was prepared from 4-bromo-5-chloro-2-methylaniline by chlorination with N-chlorosuccinimide. The product was isolated as a solid, m.p. 66°-68° C. The product was characterized by IR and 1H NMR spectroscopy and combustion analysis.

後処理

customThe product was isolated as a solid, m.p. 66°-68° C

出典と根拠

ORDレコード: ord-e046e59d76fa41bb964bf500cbd33ffd
出典データセット: uspto-grants-1989_12
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04886883

反応ノート

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