化工社化工社 化学情報印刷レポート · 研究参考用
Gamma-Butyrolactone → HCID 14997826、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Gamma-Butyrolactone | HCID 7302 | — |
| 反応物 | Hexadecylamine | HCID 8926 | — |
| 触媒 | Zincchloride | HCID 3007855 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | HCID 14997826 | HCID 14997826 | 797.2% |
反応手順
A mixture of 59.45 g of hexadecylamine, 10.60 g of gamma butyrolactone, 200 ml of toluene, and 20 mg of zinc chloride was refluxed under nitrogen for three days. Upon cooling, the reaction mixture formed a precipitate which was recrystallized twice from toluene to yield 321.5 g (78.12%) of N-hexadecyl-4-hydroxybutyramide, m.p. 89.5°-90°
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04888328 |
| 出典データセット | uspto-grants-1989_12 |
| ORD ID | ord-ace47e70aa9a437aa3253784f3fa093f |
| 出典メモ | uspto-grants-1989_12 |