化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl chloroformate → 1-Ethoxycarbonyl-1-phenythiosemicarbazide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl chloroformate | HCID 10928 | — |
| 反応物 | 1-Phenylthiosemicarbazide | HCID 2781094 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 1-Ethoxycarbonyl-1-phenythiosemicarbazide | HCID 85773191 | — |
反応手順
A mixture of 1-phenylthiosemicarbazide (25 g), ethanol (180 ml) and ethyl chloroformate (17 ml) was heated under reflux with stirring for 30 minutes. The mixture was cooled to room temperature and the solid was filtered, washed with ethanol and then with ether to give 28.9 g of the desired product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04889553 |
| 出典データセット | uspto-grants-1989_12 |
| ORD ID | ord-ec16df487b4344ac9ab14b8560048c96 |
| 出典メモ | uspto-grants-1989_12 |