化工社化工社 化学情報印刷レポート · 研究参考用
Carbonic Acid → 1-Methyl-4,6,7,8-tetrahydro-2(3H)-naphthalenone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Carbonic Acid | HCID 767 | — |
| 反応物 | Oxalic Acid | HCID 971 | — |
| 反応物 | Carvone, (+-)- | HCID 7439 | — |
| 反応物 | Cyclohexanone, 2-hydroxy- | HCID 10785 | — |
| 生成物 | 1-Methyl-4,6,7,8-tetrahydro-2(3H)-naphthalenone | HCID 19835392 | — |
反応手順
This material is prepared according to the procedure for Preparation 6 wherein 2-hydroxycyclohexanone is substituted for carvone. The resulting hydroxyketone is converted to the semicarbazone before dehydration with aqueous oxalic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04889947 |
| 出典データセット | uspto-grants-1989_12 |
| ORD ID | ord-4ec6c56119a54402927d9d281f967d94 |
| 出典メモ | uspto-grants-1989_12 |