HCID 22064513、化合物 → 498546-32-0

HRID 478688ノート

反応式

HRID 478688 の反応式
C([NH:4][C:5]1[C:6]([C:18]([OH:20])=[O:19])=[CH:7][C:8]2[C:13]([C:14]=1[N+:15]([O-:17])=[O:16])=[CH:12][CH:11]=[CH:10][CH:9]=2)(=O)C>Cl>[NH2:4][C:5]1[C:6]([C:18]([OH:20])=[O:19])=[CH:7][C:8]2[C:13]([C:14]=1[N+:15]([O-:17])=[O:16])=[CH:12][CH:11]=[CH:10][CH:9]=2

参加物

3

反応物 1

HCID 22064513HCID 22064513、化合物

生成物 1

HCID 22064531498546-32-0

試薬・触媒・溶媒 1

HCID 313Hydrochloric Acid溶媒

実験手順

A solution of 1 g of the compound obtained in Step 1 in 18 ml of hydrochloric acid is refluxed for 4 hours and then poured onto ice. The precipitate formed is filtered off, washed with water until the pH is 5-6 and then dried, allowing the expected product to be isolated.

後処理

  1. additionpoured onto ice
  2. customThe precipitate formed
  3. filtrationis filtered off
  4. washwashed with water until the pH is 5-6
  5. customdried
  6. customto be isolated

出典と根拠

ORDレコード
ord-087c1d3dd4404494aaac4f4b2d48a6b6
出典データセット
uspto-grants-2003_11
特許番号
US06642248B2

反応ノート

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