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3,5-Difluorophenylacetic acid → N-[(3,5-difluorophenyl)acetyl]alanine iso-butyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,5-Difluorophenylacetic acid | HCID 145424 | — |
| 反応物 | 2-methylpropyl (2S)-2-aminopropanoate | HCID 13743556 | — |
| 生成物 | N-[(3,5-difluorophenyl)acetyl]alanine iso-butyl ester | HCID 22894975 | — |
反応手順
Following General Procedure I above, and using 3,5-difluorophenylacetic acid (Aldrich) and alanine iso-butyl ester (prepared following General Procedure J above), the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by filtration as described in the general procedure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06642261B2 |
| 出典データセット | uspto-grants-2003_11 |
| ORD ID | ord-73a787a1914b4bb9bc3947af7df5fa92 |
| 出典メモ | uspto-grants-2003_11 |