Ammonia → 6-Hydroxyquinoline-5-carboxamide

HRID 4791

反応式

HRID 4791 の反応式
C[O:2][C:3]([C:5]1[C:6]2[CH:7]=[CH:8][CH:9]=[N:10][C:11]=2[CH:12]=[CH:13][C:14]=1[OH:15])=O.[NH3:16]>>[OH:15][C:14]1[CH:13]=[CH:12][C:11]2[N:10]=[CH:9][CH:8]=[CH:7][C:6]=2[C:5]=1[C:3]([NH2:16])=[O:2]

参加物

3

反応物 2

HCID 222Ammonia2 回HCID 19077292Methyl 6-hydroxyquinoline-5-carboxylate

生成物 1

HCID 212714806-Hydroxyquinoline-5-carboxamide

実験手順

6-Hydroxy-5-quinolinecarboxylic acid methyl ester is reacted with excess ammonia in a steel bomb for 12-18 hr. The excess ammonia is allowed to evaporate and the residue is crystallized from a suitable solvent to give the title compound.

後処理

  1. customto evaporate
  2. customthe residue is crystallized from a suitable solvent

出典と根拠

ORDレコード
ord-8364f102cacd4f039922a83884184b50
出典データセット
uspto-grants-1988_02
特許番号
US04727152

関連ノート

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