p-Chlorothiophenol → HCID 23693160、化合物

HRID 479884ノート

反応式

HRID 479884 の反応式
ClC1C=CC=CC=1.[Cl:8][C:9]1[CH:14]=[CH:13][C:12]([SH:15])=[CH:11][CH:10]=1.[OH-].[K+:17]>>[Cl:8][C:9]1[CH:14]=[CH:13][C:12]([S-:15])=[CH:11][CH:10]=1.[K+:17]

参加物

4

反応物 3

HCID 7815p-ChlorothiophenolHCID 7964ChlorobenzeneHCID 14797Potassium Hydroxide

生成物 1

HCID 23693160HCID 23693160、化合物

実験手順

A 4-necked, 1-liter flask equipped with a stirrer, a thermometer, a dropping funnel and a condenser tube was charged with a monochlorobenzene solution (0.871 mole of 4-chlorothiophenol) of 4-chlorothiophenol (13.3% of impurities) prepared by the process of Example 2 and 520 g (0.929 mole) of an aqueous solution of 10 wt % potassium hydroxide. The mixture was reacted at 25° C. for 15 minutes and was subjected to separation procedure to give an aqueous solution of potassium 4-chlorothiophenolate.

後処理

  1. customA 4-necked, 1-liter flask equipped with a stirrer
  2. customThe mixture was reacted at 25° C. for 15 minutes
  3. customwas subjected to separation procedure

出典と根拠

ORDレコード
ord-a571f5b52e9940179a2551b3bb20045d
出典データセット
uspto-grants-2003_11
特許番号
US06646165B2

反応ノート

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