関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | 5,12-Dihydro-2,9-dimethylquino(2,3-b)acridine-7,14-dione | HCID 70423 | — |
| 反応物 | HCID 178427422 | HCID 178427422 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Quinacridone | HCID 13976 | — |
反応手順
20 g of C.I. pigment red 122 having an average primary particle diameter of 90 nm (in which the content of metal ions having a valence of at least 2 was 450 ppm), 4 g of a commercially available dye C.I. acid red 249 and 110 g of deionized water were mixed, aqueous ammonia was added so as to adjust the pH of a mixture liquid to 9.0, and the mixture liquid was dispersed with a paint shaker in the presence of zirconia beads as media for approximately 5 hours, to obtain a water-based pigment dispersion. The obtained water-based pigment dispersion had a high viscosity and caused flocculation. Further, the water-based pigment dispersion was diluted so as to have a concentration of 3% by weight, and the diluted water-based pigment dispersion was dropped on No.2 filter paper, to show bleeding of the dye.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US06648954B2 |
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| 出典データセット | uspto-grants-2003_11 |
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| ORD ID | ord-a93018f0c5a346c381a6a0cd5b462802 |
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| 出典メモ | uspto-grants-2003_11 |
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