化工社化工社 化学情報印刷レポート · 研究参考用
N,N-Diethyl-1,3-propanediamine → 5-Nitroisophthalic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N,N-Diethyl-1,3-propanediamine | HCID 61011 | — |
| 反応物 | Dimethyl 5-nitroisophthalate | HCID 83316 | — |
| 生成物 | 5-Nitroisophthalic acid | HCID 12069 | — |
| 生成物 | 3-Diethylaminopropylamide | HCID 86585225 | — |
反応手順
Fifty parts of dimethyl 5-nitroisophthalate and 130 parts of N,N-diethyl-1,3-propanediamine were reacted for about four hours at 80 to 100° C. under a slight vacuum. After confirming the disappearance of the starting material dimethyl 5-nitroisophthalate and monoamide compounds, the excess N,N-diethyl-1,3-propanediamine was removed under vacuum, yielding 92 parts of 5-nitroisophthalic acid bis-3-diethylaminopropylamide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06653000B2 |
| 出典データセット | uspto-grants-2003_11 |
| ORD ID | ord-88c9270eb2f04da9be0c30f71a9ca05e |
| 出典メモ | uspto-grants-2003_11 |