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Uridine → 5'-O-(4-Methylbenzoyl)uridine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Uridine | HCID 6029 | — |
| 反応物 | 4-Methylbenzoyl Chloride | HCID 13405 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | 5'-O-(4-Methylbenzoyl)uridine | HCID 11588577 | — |
反応手順
4-Methylbenzoyl chloride (10 mmol) is added to a solution of uridine (10 mmol) in 20 mL of pyridine. After no further progress occurs as observed by TLC, the volatile components are evaporated in vacuo. The residue is purified using flash chromatography to give the product as a colorless oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06702705B1 |
| 出典データセット | uspto-grants-2004_03 |
| ORD ID | ord-5fea9a53770246ee989f9ac9adc592d9 |
| 出典メモ | uspto-grants-2004_03 |