関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Undecylenic Acid | HCID 5634 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 生成物 | Potassium Undecylenate | HCID 23692638 | — |
反応手順
Undecylenic acid (18.8 g, 0.102 mol) was added dropwise gradually to ½ N ethanolic solution of potassium hydroxide (200 mL) with stirring at 0° C. The volatile matter was distilled off under reduced pressure to give a crude product. The crude product was washed with acetone and heated under reduced pressure to give potassium undecylenate represented by the formula given below as a white solid (8.88 g, yield 88%). CH2═CH—(CH2)8—CO2−K+
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06653429B1 |
|---|
| 出典データセット | uspto-grants-2003_11 |
|---|
| ORD ID | ord-1b4321c7bf194dfda01bad07d89390e2 |
|---|
| 出典メモ | uspto-grants-2003_11 |
|---|
