化工社化工社 化学情報印刷レポート · 研究参考用
Phthalonitrile → 1,4-Benzenedimethanamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phthalonitrile | HCID 7042 | — |
| 反応物 | 1,4-Cyclohexanedimethanamine | HCID 17354 | — |
| 生成物 | 1,4-Benzenedimethanamine | HCID 68315 | — |
反応手順
It is known to prepare 1,4-bis(aminomethyl)cyclohexane from dicyanobenzene in a two stage process as disclosed, e.g., in DE-A 3,003,730. In the first stage dicyanobenzene is catalytically hydrogenated to produce 1,4-bis(aminomethyl)benzene, which is then catalytically hydrogenated to produce 1,4-bis(aminomethyl)cyclohexane. One disadvantage is that the starting material must be produced with hydrogen cyanide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05789620 |
| 出典データセット | uspto-grants-1998_08 |
| ORD ID | ord-df5237de56f24ca5928ad22d0782c545 |
| 出典メモ | uspto-grants-1998_08 |