化工社化工社 化学情報印刷レポート · 研究参考用
Benzylamine → N-Benzyl-2-chloro-9-isopropyl-9H-purin-6-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzylamine | HCID 7504 | — |
| 反応物 | 2,6-dichloro-9-(propan-2-yl)-9H-purine | HCID 11218490 | — |
| 溶媒 | 1-Butanol | HCID 263 | — |
| 生成物 | N-Benzyl-2-chloro-9-isopropyl-9H-purin-6-amine | HCID 10733091 | 85% |
反応手順
2,6-dichloro-9-isopropylpurine (1 mmol) and benzylamine (3.5 mmol) were heated with stirring in 3 ml of n-butanol (3 hour, 110° C.). The reaction mixture (after evaporation of n-butanol) was worked up as above for the compound 2, yield 85-90%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06703395B2 |
| 出典データセット | uspto-grants-2004_03 |
| ORD ID | ord-d2bcde2ca2704df1811ca52f0c53f035 |
| 出典メモ | uspto-grants-2004_03 |