関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ammonium nitrate | HCID 22985 | — |
| 反応物 | Bentazone-sodium | HCID 13124860 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Bentazone ammonium | HCID 131720800 | 73.2% |
反応手順
8 g of ammonium nitrate were introduced at 50° C. with stirring into a solution of 26.3 g of bentazone-sodium in 21.7 g of water, and the reaction mixture was subsequently stirred for a further hour. After cooling to 20° C., the precipitate was filtered off, washed twice with 5 ml of ice water in each case and dried under reduced pressure and at 50° C. 18.9 g of bentazone-ammonium of 99% purity were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US05795983 |
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| 出典データセット | uspto-grants-1998_08 |
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| ORD ID | ord-7473581cb0484df3816afca8d4efcaec |
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| 出典メモ | uspto-grants-1998_08 |
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